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by monomers of synthetic polymer has become a valuable tool to set up stable interactions between macromolecules. For instance, cross-linking by reaction with acrylic acid derivatives is a well-known method of imparting thermo-set character in elastomers. Similarly, cross-linking by reaction with polyurethane yields composites with improved mechanical properties. Furthermore, this particular type of cross-linking has recently been used to prepare microporous films having soft membranes. In contrast, cross-linking by reaction with alkylene oxides is less known. More specifically, ethylene oxide is either incorporated in the synthetic polymer or the polymer is dissolved in a solution of ethylene oxide and cured. Both processes have drawbacks. Firstly, the use of ethylene oxide as a solvent raises environmental and safety concerns. Also, since ethylene oxide is highly reactive and hydrolyzes to ethylene glycol, a side-product, it is inconvenient to implement a polymer synthesis in the presence of ethylene oxide.
Although the use of ethylene oxide may be improved, it can be achieved only at the expense of the cross-linking reaction. Therefore, it is an object of the present invention to provide a method for achieving cross-linking by reaction with alkylene oxides that involves a low use of the reactive monomer. The use of lower amounts of the monomer in the cross-linking reaction necessitates the preparation of a solution of the synthetic polymer and of the monomer. One strategy which has been used to achieve this is to conduct the cross-linking in a reactive solvent. However, reactive solvents such as ethylene oxide generally exhibit other disadvantages when used as solvent, such as corrosion, inflammability and explosivity.
Therefore, it is a further object of the present invention to provide a cross-linking method that does not require the use of highly reactive solvents such as ethylene oxide. Furthermore, it is an object of the present invention to provide a method for cross-linking in which the use of reactive solvents is minimized, or even avoided.
It has now been surprisingly found that these objects can be met by the cross-linking of a
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